LCMS:Hochuekkito
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(Redirected from Hochuekkito LC-MS)
LCMS Data List |
Names |
2D-Mass chromatogram
Analytical conditions (Negative mode)
Instrument | Shimadzu LC-IT-TOF MS ESI |
Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
Column temperature | 40 °C |
Solvent A | 5 mM Ammonium acetate solution |
Solvent B | acetonitrile |
Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
Source voltage | -3.5 kV |
Capillary temperature | 200 °C |
Nebulizer gas | 1.5 l/min |
Retention Time (min) | Compounds | Origin | Molecular formula | (M-H)- ions |
---|---|---|---|---|
8.33 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
8.59 | Dihydroxyflavanone-glucopyranoside | Glycyrrhizae | C21H21O9 | 417.1150 |