LCMS:Astragali Radix
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LCMS Data List |
Names |
TIC
Analytical conditions (Positive mode)
Instrument | Shimadzu LC-IT-TOF MS ESI |
Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
Column temperature | 40 °C |
Solvent A | 5 mM Ammonium acetate solution |
Solvent B | acetonitrile |
Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
Source voltage | 4.5 kV |
Capillary temperature | 200 °C |
Nebulizer gas | 1.5 l/min |
Analytical conditions (Negative mode)
Instrument | Shimadzu LC-IT-TOF MS ESI |
Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
Column temperature | 40 °C |
Solvent A | 5 mM Ammonium acetate solution |
Solvent B | acetonitrile |
Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
Source voltage | -3.5 kV |
Capillary temperature | 200 °C |
Nebulizer gas | 1.5 l/min |