LCMS:Yokukansan

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== <span style="color:blue"> Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”==
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;Article Title
[[Image:Yokukann1.jpg|thumb|900px|center|<big><big>LC-MS TIC of extracts</big></big>]]
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: “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
[[Image:Yokukann2.jpg|thumb|900px|center|<big><big>LC-MS TIC of standard compounds</big></big>]]
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;Authors
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: Yamada et.al
  
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==TIC==
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[[Image:Yokukann1.jpg|thumb|700px|center|LC-MS TIC of extracts]]
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[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]]
  
== <span style="color:blue"> Analytical conditions ==
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==Analytical conditions==
 
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== <span style="color:blue"> LC-MS raw data==
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==LC-MS raw data==
  
 
===Yokukansan (Tumura)===
 
===Yokukansan (Tumura)===

Revision as of 13:33, 6 January 2011

Article Title
“Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
Authors
Yamada et.al

Contents

TIC

LC-MS TIC of extracts
LC-MS TIC of standard compounds

Analytical conditions

Instrument Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
Column Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column Temperature 40℃
Solvent A 5 mM Ammonium acetate solution
Solvent B acetonitrile
Gradient 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage 4.5 kV
Capillary temperature 200 °C
Nebulizer gas 1.5 l/min


LC-MS raw data

Yokukansan (Tumura)

Yokukansan (prepared in our Lab.)

Uncaria-free Yokukansan (prepared in our Lab.)

Uncaria extract (prepared in our Lab.)

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