LCMS:Yokukansan

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== <span style="color:blue"> Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”==
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{{LCMS/Header}}
[[Image:Yokukann1.jpg|thumb|900px|left|<big><big>LC-MS TIC of extracts</big></big>]]
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{{CrudeDrug/TIC
[[Image:Yokukann2.jpg|thumb|900px|left||<big><big>LC-MS TIC of standard compounds</big></big>]]
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|TICFile=Yokukann_rev
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}}
  
== <span style="color:blue"> Analytical conditions ==
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{{CrudeDrug/TIC
{| class="wikitable" style="width:80%"
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|TICFile=Yokukann2
|-
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}}
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
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|-
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{{CrudeDrug/LCMS/Pos
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
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|PInstrument =Shimadzu LC-IT-TOF MS ESI
|-
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|PColumn    =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
| Column Temperature|| 40℃ 
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|PTemperature=40
|-
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|PSolventA  =5 mM Ammonium acetate solution
| Solvent A || 5 mM Ammonium acetate solution
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|PSolventB  =acetonitrile
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|PGradient  =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
| Solvent B || acetonitrile
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|PVoltage    =4.5
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|PCapillary  =200
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
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|PGas        =1.5
|-
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}}
| Source voltage ||  4.5 kV
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|-
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==LC-MS raw data==
| Capillary temperature || 200 °C
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|-
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| Nebulizer gas || 1.5 l/min
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|}
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== <span style="color:blue"> LC-MS raw data==
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===Yokukansan (Tumura)===
 
===Yokukansan (Tumura)===

Latest revision as of 19:55, 16 March 2011

LCMS
Data List
Names

Contents

[edit] TIC

LC-MS TIC of extracts

[edit] TIC

LC-MS TIC of extracts

[edit] Analytical conditions (Positive mode)

Instrument Shimadzu LC-IT-TOF MS ESI
Column Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column temperature 40 °C
Solvent A 5 mM Ammonium acetate solution
Solvent B acetonitrile
Gradient 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage 4.5 kV
Capillary temperature 200 °C
Nebulizer gas 1.5 l/min

[edit] LC-MS raw data

[edit] Yokukansan (Tumura)

[edit] Yokukansan (prepared in our Lab.)

[edit] Uncaria-free Yokukansan (prepared in our Lab.)

[edit] Uncaria extract (prepared in our Lab.)

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