LCMS:Yokukansan

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{{LCMS/Header}}
 
{{LCMS/Header}}
;Article Title
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{{CrudeDrug/TIC
: “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
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|TICFile=Yokukann1
;Authors
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}}
: Yamada et.al
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==TIC==
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{{CrudeDrug/TIC
[[Image:Yokukann1.jpg|thumb|700px|center|LC-MS TIC of extracts]]
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|TICFile=Yokukann2
[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]]
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}}
 
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==Analytical conditions==
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{| class="wikitable" style="width:80%"
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|-
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| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
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|-
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| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
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|-
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| Column Temperature|| 40℃ 
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|-
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| Solvent A || 5 mM Ammonium acetate solution
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|-
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| Solvent B || acetonitrile
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|-
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| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
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|-
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| Source voltage ||  4.5 kV
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|-
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| Capillary temperature || 200 °C
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|-
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| Nebulizer gas || 1.5 l/min
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|}
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 +
{{CrudeDrug/LCMS/Pos
 +
|PInstrument =Shimadzu LC-IT-TOF MS ESI
 +
|PColumn    =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
 +
|PTemperature=40
 +
|PSolventA  =5 mM Ammonium acetate solution
 +
|PSolventB  =acetonitrile
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|PGradient  =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
 +
|PVoltage    =4.5
 +
|PCapillary  =200
 +
|PGas        =1.5
 +
}}
  
 
==LC-MS raw data==
 
==LC-MS raw data==

Revision as of 18:11, 14 February 2011

LCMS
Data List
Names

Contents

TIC

LC-MS TIC of extracts

TIC

LC-MS TIC of extracts

Analytical conditions (Positive mode)

Instrument Shimadzu LC-IT-TOF MS ESI
Column Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column temperature 40 °C
Solvent A 5 mM Ammonium acetate solution
Solvent B acetonitrile
Gradient 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage 4.5 kV
Capillary temperature 200 °C
Nebulizer gas 1.5 l/min

LC-MS raw data

Yokukansan (Tumura)

Yokukansan (prepared in our Lab.)

Uncaria-free Yokukansan (prepared in our Lab.)

Uncaria extract (prepared in our Lab.)

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