LCMS:Yokukansan
From Metabolomics.JP
(Difference between revisions)
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[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]] | [[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]] | ||
− | + | ==Analytical conditions== | |
− | | | + | {| class="wikitable" style="width:80%" |
− | | | + | |- |
− | | | + | | Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
− | | | + | |- |
− | | | + | | Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
− | | | + | |- |
− | | | + | | Column Temperature|| 40℃ |
− | | | + | |- |
− | | | + | | Solvent A || 5 mM Ammonium acetate solution |
− | } | + | |- |
+ | | Solvent B || acetonitrile | ||
+ | |- | ||
+ | | Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | ||
+ | |- | ||
+ | | Source voltage || 4.5 kV | ||
+ | |- | ||
+ | | Capillary temperature || 200 °C | ||
+ | |- | ||
+ | | Nebulizer gas || 1.5 l/min | ||
+ | |} | ||
+ | |||
==LC-MS raw data== | ==LC-MS raw data== |
Revision as of 18:38, 10 February 2011
- Article Title
- “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
- Authors
- Yamada et.al
Contents |
TIC
Analytical conditions
Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
Column Temperature | 40℃ |
Solvent A | 5 mM Ammonium acetate solution |
Solvent B | acetonitrile |
Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
Source voltage | 4.5 kV |
Capillary temperature | 200 °C |
Nebulizer gas | 1.5 l/min |