LCMS:Yokukansan

From Metabolomics.JP
(Difference between revisions)
Jump to: navigation, search
Line 8: Line 8:
 
[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]]
 
[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]]
  
==Analytical conditions==
 
 
{{{CrudeDrug/LCMS/Pos
 
{{{CrudeDrug/LCMS/Pos
 
|PInstrument =Shimadzu LC-IT-TOF MS ESI
 
|PInstrument =Shimadzu LC-IT-TOF MS ESI

Revision as of 18:37, 10 February 2011

Article Title
“Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
Authors
Yamada et.al

Contents

TIC

LC-MS TIC of extracts
LC-MS TIC of standard compounds

{===Analytical conditions (Positive mode)===

Instrument Shimadzu LC-IT-TOF MS ESI
Column Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column temperature 40 °C
Solvent A 5 mM Ammonium acetate solution
Solvent B acetonitrile
Gradient 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage 4.5 kV
Capillary temperature 200 °C
Nebulizer gas 1.5 l/min

LC-MS raw data

Yokukansan (Tumura)

Yokukansan (prepared in our Lab.)

Uncaria-free Yokukansan (prepared in our Lab.)

Uncaria extract (prepared in our Lab.)

Personal tools
Namespaces

Variants
Actions
Navigation
metabolites
Toolbox