LCMS:Yokukansan

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== <span style="color:blue"> Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”==
 
== <span style="color:blue"> Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”==
 
[[Image:Yokukann1.jpg|thumb|800px|left|<big><big>LC-MS TIC of extracts</big></big>]]
 
[[Image:Yokukann1.jpg|thumb|800px|left|<big><big>LC-MS TIC of extracts</big></big>]]
[[Image:Yokukann2.jpg|thumb|800px|left|LC-MS TIC of standard compounds]]
+
[[Image:Yokukann2.jpg|thumb|800px|left||<big><big>LC-MS TIC of standard compounds</big></big>]]
  
 
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Revision as of 12:52, 16 December 2010

Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”

LC-MS TIC of extracts
LC-MS TIC of standard compounds
Instrument Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
Column Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column Temperature 40℃
Solvent A 5 mM Ammonium acetate solution
Solvent B acetonitrile
Gradient 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage 4.5 kV
Capillary temperature 200 °C
Nebulizer gas 1.5 l/min
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