LCMS:Linderae Radix
From Metabolomics.JP
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==TIC== | ==TIC== | ||
| − | [[Image: | + | [[Image:Linderae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]] |
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==Analytical conditions== | ==Analytical conditions== | ||
Revision as of 09:51, 2 February 2011
Contents |
TIC
Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
