LCMS:Hochuekkito
From Metabolomics.JP
2D-Mass chromatogram
| Instrument | Shimadzu LC-IT-TOF MS ESI (Negative ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | – 3.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
| Retention Time (min) | Compounds | Origin | Molecular formula | (M-H)- ions |
|---|---|---|---|---|
| 8.33 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 8.59 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 8.75 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 8.97 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 9.19 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 9.49 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 10.20 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 10.43 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 11.08 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 11.31 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 11.51 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 11.65 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 12.02 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 12.36 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 12.57 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 12.60 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.12 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.18 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.31 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.40 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.65 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.64 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.76 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 13.99 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 14.23 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 14.48 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 14.71 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 14.95 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 15.70 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 16.06 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 16.13 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 17.87 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 18.88 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 19.11 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 19.19 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 20.73 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 21.39 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 22.13 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 22.73 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 23.53 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 23.75 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 24.73 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 24.81 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 25.15 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
| 26.58 | Trihydroxyflavone-diglucopyranoside | Aurantii Nobilis | C27H29O15 | 593.1495 |
