LCMS:Yokukansan
From Metabolomics.JP
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===Yokukansan (prepared in our Lab.)=== | ===Yokukansan (prepared in our Lab.)=== | ||
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===Uncaria-free Yokukansan (prepared in our Lab.)=== | ===Uncaria-free Yokukansan (prepared in our Lab.)=== | ||
Revision as of 13:29, 16 December 2010
Contents |
Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
