LCMS:Yokukansan
From Metabolomics.JP
(Difference between revisions)
| Line 8: | Line 8: | ||
[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]] | [[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]] | ||
| − | |||
{{{CrudeDrug/LCMS/Pos | {{{CrudeDrug/LCMS/Pos | ||
|PInstrument =Shimadzu LC-IT-TOF MS ESI | |PInstrument =Shimadzu LC-IT-TOF MS ESI | ||
Revision as of 18:37, 10 February 2011
- Article Title
- “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
- Authors
- Yamada et.al
Contents |
TIC
{===Analytical conditions (Positive mode)===
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |