LCMS:Yokukansan
From Metabolomics.JP
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[[Image:Yokukann2.jpg|thumb|900px|left||<big><big>LC-MS TIC of standard compounds</big></big>]] | [[Image:Yokukann2.jpg|thumb|900px|left||<big><big>LC-MS TIC of standard compounds</big></big>]] | ||
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Revision as of 14:13, 16 December 2010
Contents |
Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
