LCMS:Yokukansan

Latest revision as of 19:55, 16 March 2011

LC-MS TIC of extracts

LC-MS TIC of extracts

Instrument	Shimadzu LC-IT-TOF MS ESI
Column	Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
Column temperature	40 °C
Solvent A	5 mM Ammonium acetate solution
Solvent B	acetonitrile
Gradient	10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
Source voltage	4.5 kV
Capillary temperature	200 °C
Nebulizer gas	1.5 l/min

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-== <span style="color:blue"> Supplement data for the manuscript, Yamada et.al., “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”==
+{{LCMS/Header}}
-[[Image:Yokukann1.jpg|thumb|900px|left|<big><big>LC-MS TIC of extracts</big></big>]]
+{{CrudeDrug/TIC
-[[Image:Yokukann2.jpg|thumb|900px|left||<big><big>LC-MS TIC of standard compounds</big></big>]]
+|TICFile=Yokukann_rev
+}}
-== <span style="color:blue"> Analytical conditions ==
+{{CrudeDrug/TIC
-{| class="wikitable" style="width:80%"
+|TICFile=Yokukann2
-|-
+}}
-| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
-|-
+{{CrudeDrug/LCMS/Pos
-| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
+|PInstrument =Shimadzu LC-IT-TOF MS ESI
-|-
+|PColumn     =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
-| Column Temperature|| 40℃
+|PTemperature=40
-|-
+|PSolventA   =5 mM Ammonium acetate solution
-| Solvent A || 5 mM Ammonium acetate solution
+|PSolventB   =acetonitrile
-|-
+|PGradient   =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-| Solvent B || acetonitrile
+|PVoltage    =4.5
-|-
+|PCapillary  =200
-| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
+|PGas        =1.5
-|-
+}}
-| Source voltage ||  4.5 kV
-|-
+==LC-MS raw data==
-| Capillary temperature || 200 °C
-|-
-| Nebulizer gas || 1.5 l/min
-|}
-== <span style="color:blue"> LC-MS raw data==
 ===Yokukansan (Tumura)===