LCMS:Yokukansan
From Metabolomics.JP
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| − | + | {{LCMS/Header}} | |
| − | + | {{CrudeDrug/TIC | |
| − | + | |TICFile=Yokukann_rev | |
| + | }} | ||
| − | {| | + | {{CrudeDrug/TIC |
| − | + | |TICFile=Yokukann2 | |
| − | | | + | }} |
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| − | + | {{CrudeDrug/LCMS/Pos | |
| − | | | + | |PInstrument =Shimadzu LC-IT-TOF MS ESI |
| − | | | + | |PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| − | + | |PTemperature=40 | |
| − | + | |PSolventA =5 mM Ammonium acetate solution | |
| − | | | + | |PSolventB =acetonitrile |
| − | + | |PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | |
| − | | | + | |PVoltage =4.5 |
| − | + | |PCapillary =200 | |
| − | | | + | |PGas =1.5 |
| − | + | }} | |
| − | | | + | |
| − | + | ==LC-MS raw data== | |
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| − | == | + | |
===Yokukansan (Tumura)=== | ===Yokukansan (Tumura)=== | ||
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===Uncaria-free Yokukansan (prepared in our Lab.)=== | ===Uncaria-free Yokukansan (prepared in our Lab.)=== | ||
| − | {{JCampViewer| | + | {{JCampViewer|Yokukan_UF.gz}} |
===Uncaria extract (prepared in our Lab.)=== | ===Uncaria extract (prepared in our Lab.)=== | ||
| − | {{JCampViewer| | + | {{JCampViewer|Uncaria.gz}} |
Latest revision as of 19:55, 16 March 2011
| LCMS Data List |
Names |
Contents |
[edit] TIC
[edit] TIC
[edit] Analytical conditions (Positive mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
