LCMS:Yokukansan
From Metabolomics.JP
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| + | {{CrudeDrug/LCMS/Pos | ||
| + | |PInstrument =Shimadzu LC-IT-TOF MS ESI | ||
| + | |PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) | ||
| + | |PTemperature=40 | ||
| + | |PSolventA =5 mM Ammonium acetate solution | ||
| + | |PSolventB =acetonitrile | ||
| + | |PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | ||
| + | |PVoltage =4.5 | ||
| + | |PCapillary =200 | ||
| + | |PGas =1.5 | ||
| + | }} | ||
==LC-MS raw data== | ==LC-MS raw data== | ||
Revision as of 18:11, 14 February 2011
| LCMS Data List |
Names |
Contents |
TIC
TIC
Analytical conditions (Positive mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
