LCMS:Yokukansan
From Metabolomics.JP
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==Analytical conditions== | ==Analytical conditions== | ||
| − | {| | + | {{{CrudeDrug/LCMS/Pos |
| − | + | |PInstrument =Shimadzu LC-IT-TOF MS ESI | |
| − | + | |PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) | |
| − | | | + | |PTemperature=40 |
| − | + | |PSolventA =5 mM Ammonium acetate solution | |
| − | | | + | |PSolventB =acetonitrile |
| − | | | + | |PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | + | |PVoltage =4.5 | |
| − | + | |PCapillary =200 | |
| − | | | + | |PGas =1.5 |
| − | + | }} | |
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==LC-MS raw data== | ==LC-MS raw data== | ||
Revision as of 18:36, 10 February 2011
- Article Title
- “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
- Authors
- Yamada et.al
Contents |
TIC
Analytical conditions
{===Analytical conditions (Positive mode)===
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
