LCMS:Salviae miltiorhizae Radix
From Metabolomics.JP
(Difference between revisions)
(New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-...) |
|||
| (3 intermediate revisions by one user not shown) | |||
| Line 1: | Line 1: | ||
| − | + | {{LCMS/Header}} | |
| − | + | {{CrudeDrug/TIC | |
| + | |TICFile=Salviae miltiorhizae LC-MS | ||
| + | }} | ||
| − | + | {{CrudeDrug/LCMS/Pos | |
| − | + | |PInstrument =Shimadzu LC-IT-TOF MS ESI | |
| − | + | |PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) | |
| − | + | |PTemperature=40 | |
| − | | | + | |PSolventA =5 mM Ammonium acetate solution |
| − | + | |PSolventB =acetonitrile | |
| − | | | + | |PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | | | + | |PVoltage =4.5 |
| − | + | |PCapillary =200 | |
| − | + | |PGas =1.5 | |
| − | | | + | }} |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | + | ||
| − | {| | + | {{CrudeDrug/LCMS/Neg |
| − | + | |NInstrument =Shimadzu LC-IT-TOF MS ESI | |
| − | + | |NColumn =Waters Atlantis T3 (2.1 mm x 150 mm) | |
| − | | | + | |NTemperature=40 |
| − | + | |NSolventA =5 mM Ammonium acetate solution | |
| − | | | + | |NSolventB =acetonitrile |
| − | | | + | |NGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | + | |NVoltage =-3.5 | |
| − | + | |NCapillary =200 | |
| − | | | + | |NGas =1.5 |
| − | + | }} | |
| − | | | + | |
| − | + | ||
| − | |- | + | |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | | | + | |
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | ||
Latest revision as of 16:34, 14 February 2011
| LCMS Data List |
Names |
[edit] TIC
[edit] Analytical conditions (Positive mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
[edit] Analytical conditions (Negative mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | -3.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
