LCMS:Salviae miltiorhizae Radix
From Metabolomics.JP
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(New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-...) |
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| − | + | |PInstrument =Shimadzu LC-IT-TOF MS ESI | |
| − | + | |PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) | |
| − | + | |PTemperature=40 | |
| − | | | + | |PSolventA =5 mM Ammonium acetate solution |
| − | + | |PSolventB =acetonitrile | |
| − | | | + | |PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | | | + | |PVoltage =4.5 |
| − | + | |PCapillary =200 | |
| − | + | |PGas =1.5 | |
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| − | {| | + | {{CrudeDrug/LCMS/Neg |
| − | + | |NInstrument =Shimadzu LC-IT-TOF MS ESI | |
| − | + | |NColumn =Waters Atlantis T3 (2.1 mm x 150 mm) | |
| − | | | + | |NTemperature=40 |
| − | + | |NSolventA =5 mM Ammonium acetate solution | |
| − | | | + | |NSolventB =acetonitrile |
| − | | | + | |NGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | + | |NVoltage =-3.5 | |
| − | + | |NCapillary =200 | |
| − | | | + | |NGas =1.5 |
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Revision as of 18:14, 10 February 2011
TIC
[[Image::Salviae miltiorhizae LC-MS.jpg|thumb|700px|center| LC-MS TIC of extracts]]Analytical conditions (Positive mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
Analytical conditions (Negative mode)
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | -3.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
