LCMS:Linderae Radix
From Metabolomics.JP
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==LC-MS raw data== | ==LC-MS raw data== | ||
| − | === | + | ===Linderae Radix LC-MS=== |
{{JCampViewer|Linderae LC-MS.gz}} | {{JCampViewer|Linderae LC-MS.gz}} | ||
Revision as of 10:03, 2 February 2011
Contents |
TIC
Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
| Instrument | Shimadzu LC-IT-TOF MS ESI (Negative ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | – 3.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
