LCMS:Linderae Radix
From Metabolomics.JP
(Difference between revisions)
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| Nebulizer gas || 1.5 l/min | | Nebulizer gas || 1.5 l/min | ||
|} | |} | ||
| + | |||
| + | {| class="wikitable" style="width:80%" | ||
| + | |- | ||
| + | | Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode) | ||
| + | |- | ||
| + | | Column || Waters Atlantis T3 (2.1 mm x 150 mm) | ||
| + | |- | ||
| + | | Column Temperature|| 40℃ | ||
| + | |- | ||
| + | | Solvent A || 5 mM Ammonium acetate solution | ||
| + | |- | ||
| + | | Solvent B || acetonitrile | ||
| + | |- | ||
| + | | Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | ||
| + | |- | ||
| + | | Source voltage || – 3.5 kV | ||
| + | |- | ||
| + | | Capillary temperature || 200 °C | ||
| + | |- | ||
| + | | Nebulizer gas || 1.5 l/min | ||
| + | |} | ||
| + | |||
| + | |||
Revision as of 09:53, 2 February 2011
Contents |
TIC
Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
| Instrument | Shimadzu LC-IT-TOF MS ESI (Negative ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | – 3.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
