LCMS:Albizzae Cortex
From Metabolomics.JP
(Difference between revisions)
(New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS E...) |
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| − | + | {{CrudeDrug/TIC | |
| − | + | |TICFile=Albizziae LC-MS | |
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| − | + | {{CrudeDrug/LCMS/Pos | |
| − | { | + | |Instrument =Shimadzu LC-IT-TOF MS ESI |
| − | + | |Column =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) | |
| − | | Instrument | + | |Temperature=40 |
| − | + | |Solvent A =5 mM Ammonium acetate solution | |
| − | | Column | + | |Solvent B =acetonitrile |
| − | | | + | |Gradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| − | + | |Voltage =4.5 | |
| − | + | |Capillary =200 | |
| − | | Solvent A | + | |Gas =1.5 |
| − | + | }} | |
| − | | Solvent B | + | |
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| − | | Gradient | + | |
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| − | | Capillary | + | |
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| − | { | + | {{CrudeDrug/LCMS/Neg |
| − | + | |Instrument =Shimadzu LC-IT-TOF MS ESI | |
| − | | Instrument | + | |Column =Waters Atlantis T3 (2.1 mm x 150 mm) |
| − | + | |Temperature=40 | |
| − | | Column | + | |Solvent A =5 mM Ammonium acetate solution |
| − | | | + | |Solvent B =acetonitrile |
| − | + | |Gradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | |
| − | + | |Voltage =-3.5 | |
| − | | Solvent A | + | |Capillary =200 |
| − | + | |Gas =1.5 | |
| − | | Solvent B | + | }} |
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| − | | Gradient | + | |
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| − | | Capillary | + | |
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Revision as of 13:11, 10 February 2011
TIC
Analytical conditions (Positive mode)
| Instrument | {{{PInstrument}}} |
| Column | {{{PColumn}}} |
| Column temperature | {{{PTemperature}}} °C |
| Solvent A | {{{PSolventA}}} |
| Solvent B | {{{PSolventB}}} |
| Gradient | {{{PGradient}}} |
| Source voltage | {{{PVoltage}}} kV |
| Capillary temperature | {{{PCapillary}}} °C |
| Nebulizer gas | {{{PGas}}} l/min |
Analytical conditions (Negative mode)
| Instrument | {{{NInstrument}}} |
| Column | {{{NColumn}}} |
| Column temperature | {{{NTemperature}}} °C |
| Solvent A | {{{NSolventA}}} |
| Solvent B | {{{NSolventB}}} |
| Gradient | {{{NGradient}}} |
| Source voltage | {{{NVoltage}}} kV |
| Capillary temperature | {{{NCapillary}}} °C |
| Nebulizer gas | {{{NGas}}} l/min |
