View source for LCMS:Uncariae Uncis cum Ramulus

==TIC==
[[Image:Uncariae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|- 
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|- 
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃  
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage ||  4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|- 
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|- 
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃  
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}




==LC-MS raw data==

===Uncariae Uncis cum Ramulus LC-MS===
{{JCampViewer|Uncariae LC-MS.gz}}