LCMS:Linderae Radix - Revision history

Editor at 07:21, 14 February 2011

2011-02-14T07:21:49Z

Editor: moved Linderae Radix LC-MS to LCMS:Linderae Radix

2011-02-14T06:41:50Z

moved Linderae Radix LC-MS to LCMS:Linderae Radix

Editor at 08:46, 10 February 2011

2011-02-10T08:46:13Z

Toyama at 01:03, 2 February 2011

2011-02-02T01:03:19Z

Toyama at 00:55, 2 February 2011

2011-02-02T00:55:02Z

Toyama at 00:53, 2 February 2011

2011-02-02T00:53:13Z

Toyama at 00:51, 2 February 2011

2011-02-02T00:51:57Z

Toyama at 00:44, 2 February 2011

2011-02-02T00:44:27Z

Toyama: New page: ;Article Title : “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.” ;Authors : Yamada et.al ==TIC== [[Image:Yokukann1.jpg|thumb|700p...

2011-02-02T00:43:26Z

New page: ;Article Title : “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.” ;Authors : Yamada et.al ==TIC== [[Image:Yokukann1.jpg|thumb|700p...

New page

;Article Title
: “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
;Authors
: Yamada et.al

==TIC==
[[Image:Yokukann1.jpg|thumb|700px|center|LC-MS TIC of extracts]]
[[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Yokukansan (Tumura)===
{{JCampViewer|Yokukan_tumura.gz}}

← Older revision		Revision as of 07:21, 14 February 2011
Line 1:		Line 1:
		+	{{LCMS/Header}}
	{{CrudeDrug/TIC		{{CrudeDrug/TIC
	\|TICFile=Linderae LC-MS		\|TICFile=Linderae LC-MS

@@ Line 1: / Line 1: @@
-==TIC==
+{{CrudeDrug/TIC
-[[Image:Linderae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]
+|TICFile=Linderae LC-MS
-==Analytical conditions==
+{{CrudeDrug/LCMS/Pos
-{| class="wikitable" style="width:80%"
+|PInstrument =Shimadzu LC-IT-TOF MS ESI
-|-
+|PColumn     =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
-| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
+|PTemperature=40
-|-
+|PSolventA   =5 mM Ammonium acetate solution
-| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
+|PSolventB   =acetonitrile
-|-
+|PGradient   =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-| Column Temperature|| 40℃
+|PVoltage    =4.5
-|-
+|PCapillary  =200
-| Solvent A || 5 mM Ammonium acetate solution
+|PGas        =1.5
-|-
+}}
-| Solvent B || acetonitrile
-|-
-| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-|-
-| Source voltage ||  4.5 kV
-|-
-| Capillary temperature || 200 °C
-|-
-| Nebulizer gas || 1.5 l/min
-|}
-{| class="wikitable" style="width:80%"
+{{CrudeDrug/LCMS/Neg
-|-
+|NInstrument =Shimadzu LC-IT-TOF MS ESI
-| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
+|NColumn     =Waters Atlantis T3 (2.1 mm x 150 mm)
-|-
+|NTemperature=40
-| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
+|NSolventA   =5 mM Ammonium acetate solution
-|-
+|NSolventB   =acetonitrile
-| Column Temperature|| 40℃
+|NGradient   =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-|-
+|NVoltage    =-3.5
-| Solvent A || 5 mM Ammonium acetate solution
+|NCapillary  =200
-|-
+|NGas        =1.5
-| Solvent B || acetonitrile
+}}
-|-
-| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
 |-
-| Source voltage || – 3.5 kV
-|-
-| Capillary temperature || 200 °C
-|-
-| Nebulizer gas || 1.5 l/min
-|}
-−
-−
-−
-−
-==LC-MS raw data==
-−
-===Linderae Radix LC-MS===
-{{JCampViewer|Linderae LC-MS.gz}}

@@ Line 50: / Line 50: @@
 ==LC-MS raw data==
-===Yokukansan (Tumura)===
+===Linderae Radix LC-MS===
 {{JCampViewer|Linderae LC-MS.gz}}

← Older revision		Revision as of 00:55, 2 February 2011
Line 51:		Line 51:

	===Yokukansan (Tumura)===		===Yokukansan (Tumura)===
−	{{JCampViewer\|~~Yokukan_tumura~~.gz}}	+	{{JCampViewer\|Linderae LC-MS.gz}}

← Older revision		Revision as of 00:44, 2 February 2011
Line 1:		Line 1:
−	~~;Article Title~~
−	~~: “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”~~
−	~~;Authors~~
−	~~: Yamada et.al~~

	==TIC==		==TIC==

← Older revision		Revision as of 00:53, 2 February 2011
Line 23:		Line 23:
	\| Nebulizer gas \|\| 1.5 l/min		\| Nebulizer gas \|\| 1.5 l/min
	\|}		\|}
		+
		+	{\| class="wikitable" style="width:80%"
		+	\|-
		+	\| Instrument \|\| Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
		+	\|-
		+	\| Column \|\| Waters Atlantis T3 (2.1 mm x 150 mm)
		+	\|-
		+	\| Column Temperature\|\| 40℃
		+	\|-
		+	\| Solvent A \|\| 5 mM Ammonium acetate solution
		+	\|-
		+	\| Solvent B \|\| acetonitrile
		+	\|-
		+	\| Gradient \|\| 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
		+	\|-
		+	\| Source voltage \|\| – 3.5 kV
		+	\|-
		+	\| Capillary temperature \|\| 200 °C
		+	\|-
		+	\| Nebulizer gas \|\| 1.5 l/min
		+	\|}
		+
		+