Metabolomics.JP - User contributions [en]

File:Yokukann rev.jpg

2011-03-16T10:56:38Z

Toyama:

LCMS:Yokukansan

2011-03-16T10:55:55Z

Toyama:

{{LCMS/Header}}
{{CrudeDrug/TIC
|TICFile=Yokukann_rev
}}

{{CrudeDrug/TIC
|TICFile=Yokukann2
}}

{{CrudeDrug/LCMS/Pos
|PInstrument =Shimadzu LC-IT-TOF MS ESI
|PColumn =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|PTemperature=40
|PSolventA =5 mM Ammonium acetate solution
|PSolventB =acetonitrile
|PGradient =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|PVoltage =4.5
|PCapillary =200
|PGas =1.5
}}

==LC-MS raw data==

===Yokukansan (Tumura)===
{{JCampViewer|Yokukan_tumura.gz}}

===Yokukansan (prepared in our Lab.)===
{{JCampViewer|Yokukan_HM.gz}}

===Uncaria-free Yokukansan (prepared in our Lab.)===
{{JCampViewer|Yokukan_UF.gz}}

===Uncaria extract (prepared in our Lab.)===
{{JCampViewer|Uncaria.gz}}

LCMS:Psoraleae Semen

2011-02-10T02:21:20Z

Toyama:

==TIC==
[[Image:Psoraleae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Psoraleae Semen LC-MS===
{{JCampViewer|Psoraleae LC-MS.gz}}

File:Psoraleae LC-MS.jpg

2011-02-10T02:19:53Z

Toyama:

LCMS:Alismatis Rhizoma

2011-02-10T02:16:05Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (P..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Alismatis Rhizoma LC-MS===
{{JCampViewer|Alismatis LC-MS.gz}}

File:Alismatis LC-MS.gz

2011-02-10T02:15:45Z

Toyama:

LCMS:Zizyphi Fructus

2011-02-10T02:12:14Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Zizyphi Fructus LC-MS===
{{JCampViewer|Zizyphi FructusLC-MS.gz}}

File:Zizyphi FructusLC-MS.gz

2011-02-10T02:11:46Z

Toyama:

LCMS:Ganoderma

2011-02-10T01:56:51Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (P..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Ganoderma LC-MS===
{{JCampViewer|Ganoderma LC-MS.gz}}

File:Ganoderma LC-MS.gz

2011-02-10T01:56:30Z

Toyama:

LCMS:Myricae Cortex

2011-02-10T01:54:52Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Myricae Cortex LC-MS===
{{JCampViewer|Myricae LC-MS.gz}}

File:Myricae LC-MS.gz

2011-02-10T01:54:29Z

Toyama:

LCMS:Alpinae oxyphyllae Fructus

2011-02-10T01:53:00Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Alpinae oxyphyllae Fructus LC-MS===
{{JCampViewer|Alpiniae oxyphyllae LC-MS.gz}}

File:Alpiniae oxyphyllae LC-MS.gz

2011-02-10T01:52:34Z

Toyama:

LCMS:Myrrha

2011-02-10T01:45:26Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (P..."

File:Myrrha LC-MS.gz

2011-02-10T01:45:07Z

Toyama:

LCMS:Viticis Fructus

2011-02-10T01:43:37Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (Po..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Viticis Fructus LC-MS===
{{JCampViewer|Viticis LC-MS.gz}}

File:Viticis LC-MS.gz

2011-02-10T01:43:19Z

Toyama:

LCMS:Psoraleae Semen

2011-02-10T01:37:00Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI (Po..."

==TIC==
[[Image: |thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Psoraleae Semen LC-MS===
{{JCampViewer|Psoraleae LC-MS.gz}}

File:Psoraleae LC-MS.gz

2011-02-10T01:36:38Z

Toyama:

LCMS:Imperatae Rhizoma

2011-02-10T01:30:35Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-I..."

==TIC==
[[Image:Imperatae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Imperatae Rhizoma LC-MS===
{{JCampViewer|Imperatae LC-MS.gz}}

File:Imperatae LC-MS.jpg

2011-02-10T01:30:09Z

Toyama:

File:Imperatae LC-MS.gz

2011-02-10T01:28:27Z

Toyama:

File:Stemonae LC-MS.jpg

2011-02-10T01:23:24Z

Toyama: uploaded a new version of "File:Stemonae LC-MS.jpg": Reverted to version as of 01:03, 10 February 2011

LCMS:Stemonae Radix

2011-02-10T01:17:03Z

Toyama: Created page with "==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT..."

==TIC==
[[Image:Stemonae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Stemonae Radix LC-MS===
{{JCampViewer|Stemonae LC-MS.gz}}

File:Stemonae LC-MS.gz

2011-02-10T01:16:30Z

Toyama:

File:Stemonae LC-MS.jpg

2011-02-10T01:13:21Z

Toyama: uploaded a new version of "File:Stemonae LC-MS.jpg": Reverted to version as of 01:03, 10 February 2011

File:Stemonae LC-MS.jpg

2011-02-10T01:13:06Z

Toyama: uploaded a new version of "File:Stemonae LC-MS.jpg"

File:Stemonae LC-MS.jpg

2011-02-10T01:03:47Z

Toyama:

LCMS:Dictamni radicis Cortex

2011-02-08T06:58:39Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-T...

==TIC==
[[Image:Dictamni radicis LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Dictamni radicis Cortex LC-MS===
{{JCampViewer|Dictamni radicis LC-MS.gz}}

File:Dictamni radicis LC-MS.gz

2011-02-08T06:58:24Z

Toyama:

File:Dictamni radicis LC-MS.jpg

2011-02-08T06:57:49Z

Toyama:

LCMS:Cistanchis Herba

2011-02-08T06:55:45Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ...

==TIC==
[[Image:Cistanchis LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Cistanchis Herba LC-MS===
{{JCampViewer|Cistanchis LC-MS.gz}}

File:Cistanchis LC-MS.jpg

2011-02-08T06:55:30Z

Toyama:

File:Cistanchis LC-MS.gz

2011-02-08T06:54:49Z

Toyama:

LCMS:Codonopsitis Radix

2011-02-08T06:52:41Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF M...

==TIC==
[[Image:Codonopsitis LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Codonopsitis Radix LC-MS===
{{JCampViewer|Codonopsitis LC-MS.gz}}

File:Codonopsitis LC-MS.gz

2011-02-08T06:52:20Z

Toyama:

File:Codonopsitis LC-MS.jpg

2011-02-08T06:51:33Z

Toyama:

LCMS:Salviae miltiorhizae Radix

2011-02-08T06:50:37Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-...

==TIC==
[[Image:Salviae miltiorhizae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Salviae miltiorhizae Radix LC-MS===
{{JCampViewer|Salviae miltiorhizae LC-MS.gz}}

File:Salviae miltiorhizae LC-MS.jpg

2011-02-08T06:50:25Z

Toyama:

File:Salviae miltiorhizae LC-MS.gz

2011-02-08T06:49:35Z

Toyama:

LCMS:Dipsaci Radix

2011-02-08T06:48:15Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ESI...

==TIC==
[[Image:Dipsaci LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Dipsaci Radix LC-MS===
{{JCampViewer|Dipsaci LC-MS.gz}}

File:Dipsaci LC-MS.gz

2011-02-08T06:48:06Z

Toyama:

File:Dipsaci LC-MS.jpg

2011-02-08T06:47:30Z

Toyama:

LCMS:Mori Folium

2011-02-08T06:46:24Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS...

==TIC==
[[Image:Mori Folium LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Mori Folium LC-MS===
{{JCampViewer|Mori Folium LC-MS.gz}}

File:Mori Folium LC-MS.jpg

2011-02-08T06:46:13Z

Toyama:

File:Mori Folium LC-MS.gz

2011-02-08T06:45:39Z

Toyama:

LCMS:Acori-graminei

2011-02-08T06:44:33Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF...

==TIC==
[[Image:Acori-graminei LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Acori-graminei LC-MS===
{{JCampViewer|Acori-graminei LC-MS.gz}}

File:Acori-graminei LC-MS.gz

2011-02-08T06:44:19Z

Toyama:

File:Acori-graminei LC-MS.jpg

2011-02-08T06:43:32Z

Toyama:

LCMS:Artemisiae Ching-Hao Herba

2011-02-08T06:38:49Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-...

==TIC==
[[Image:Artemisiae Ching-Hao LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Artemisiae Ching-Hao Herba LC-MS===
{{JCampViewer|Artemisiae Ching-Hao LC-MS.gz}}